ISL OpenIR  > 青海盐湖研究所知识仓储
氯化锌/氯化胆碱离子液体单晶合成、表征及性质研究
邱方龙; 谢少磊; 姚颖; 景燕; 孙进贺; 贾永忠
2019
Source Publication盐湖研究
Volume27Issue:04Pages:49-54
Abstract

选用溶剂挥发法,以氯化胆碱和氯化锌为原料,成功合成了一种新型的Zn(Ⅱ)单晶[Ch][ZnCl_3],并采用单晶X射线衍射、红外光谱、X-粉末衍射、元素分析等对单晶结构进行表征。结果表明:该晶体属于单斜晶系,空间点群为P 21/c,晶胞参数a=7.322(4)?,b=9.423(5)?,c=16.688(8)?,V=1145.8(10)?~3,Z=4,C_5H_(14)Cl_3NOZn,Mr=275.89,Dc=1.599 g/cm~3,F(000)=560,m=2.797 mm~(-1),R=0.0524和wR=0.1434。通过热分析,热分解温度为323.5℃,具有较好的热稳定性,熔点为43℃,相变焓为94.1 J·cm~(-3)。

Keyword氯化锌 氯化胆碱 单晶 热分析
Language中文
Document Type期刊论文
Identifierhttp://ir.isl.ac.cn/handle/363002/15540
Collection青海盐湖研究所知识仓储
中国科学院青海盐湖研究所
Recommended Citation
GB/T 7714
邱方龙,谢少磊,姚颖,等. 氯化锌/氯化胆碱离子液体单晶合成、表征及性质研究[J]. 盐湖研究,2019,27(04):49-54.
APA 邱方龙,谢少磊,姚颖,景燕,孙进贺,&贾永忠.(2019).氯化锌/氯化胆碱离子液体单晶合成、表征及性质研究.盐湖研究,27(04),49-54.
MLA 邱方龙,et al."氯化锌/氯化胆碱离子液体单晶合成、表征及性质研究".盐湖研究 27.04(2019):49-54.
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