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Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dot H2O whiskers via a new route
Liu, Xin; Li, Wu; Nai, Xueying; Bian, Shaoju; Meng, Qingfen; Gao, Dandan; Wei, Ming
2012-04-01
发表期刊CRYSTAL RESEARCH AND TECHNOLOGY
卷号47期号:4页码:455-460
关键词Zinc Borate Whisker Synthesis Flame Retardant
摘要4ZnO.B2O3.H2O whiskers were prepared from 2ZnO.3B2O3.3.5H2O under hydrothermal process at 160 degrees C for 10 h. The synthesized product was characterized by XRD, SEM, TG-DSC and FT-IR. SEM results showed that the synthesized 4ZnO.B2O3.H2O whiskers' length was about 310 mu m and the diameter was 0.20.3 mu m. Further study on the whiskers' growth process and mechanism showed that the formation of the whiskers went through three stages and the morphology of 4ZnO.B2O3.H2O changed from irregular particles to rod-like structures and finally to whiskers. The variation of the morphology of the 4ZnO.B2O3.H2O whisker with the concentration of the starting material was investigated. (C) 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)
语种英语
引用统计
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/5557
专题青海盐湖研究所知识仓储
中国科学院青海盐湖研究所
作者单位Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining, Peoples R China
推荐引用方式
GB/T 7714
Liu, Xin,Li, Wu,Nai, Xueying,et al. Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dot H2O whiskers via a new route[J]. CRYSTAL RESEARCH AND TECHNOLOGY,2012,47(4):455-460.
APA Liu, Xin.,Li, Wu.,Nai, Xueying.,Bian, Shaoju.,Meng, Qingfen.,...&Wei, Ming.(2012).Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dot H2O whiskers via a new route.CRYSTAL RESEARCH AND TECHNOLOGY,47(4),455-460.
MLA Liu, Xin,et al."Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dot H2O whiskers via a new route".CRYSTAL RESEARCH AND TECHNOLOGY 47.4(2012):455-460.
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