Knowledge Management System Of Qinghai Institute of Salt Lakes,CAS
Determination of trace elements in salt lake brines using inductively coupled plasma optical emission spectrometry after magnesium hydroxide precipitation | |
Wang, Liping1,2; Li, Haijun1![]() ![]() ![]() ![]() ![]() | |
2015 | |
发表期刊 | ANALYTICAL METHODS
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卷号 | 7期号:19页码:8235-8240 |
摘要 | A magnesium hydroxide coprecipitation method for the determination of trace elements in high-salt samples from salt lake brines by inductively coupled plasma optical emission spectrometry (ICP-OES) was developed. Some effects on the coprecipitation and analysis, such as the pH value and Na and Mg amounts in primary brines, have been thoroughly investigated and optimized. After adjusting the pH to 8.70, associated with sodium hydroxide, the complicated matrix was removed from high salt brines, and thus trace amounts of Al, Co, Cu, Fe, Mn, Ni, V, and Zn were simultaneously coprecipitated and precisely determined. Recoveries of all the determined trace elements in the samples of both synthesized and real salt lake brines were more than 90%. The detection limit in the range of 0.62-14.4 mg L-1 was obtained and the precision was less than 3% relative standard deviation. The optimized method has been successfully applied for the determination of trace elements in the intercrystal brine mined from Dachaidan salt lake located in the Qaidam Basin, China. |
语种 | 英语 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.isl.ac.cn/handle/363002/6157 |
专题 | 青海盐湖研究所知识仓储 中国科学院青海盐湖研究所 盐湖资源综合利用工程技术中心 |
作者单位 | 1.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China 2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China |
推荐引用方式 GB/T 7714 | Wang, Liping,Li, Haijun,Dong, Yaping,et al. Determination of trace elements in salt lake brines using inductively coupled plasma optical emission spectrometry after magnesium hydroxide precipitation[J]. ANALYTICAL METHODS,2015,7(19):8235-8240. |
APA | Wang, Liping,Li, Haijun,Dong, Yaping,Peng, Jiaoyu,Feng, Haitao,&Li, Wu.(2015).Determination of trace elements in salt lake brines using inductively coupled plasma optical emission spectrometry after magnesium hydroxide precipitation.ANALYTICAL METHODS,7(19),8235-8240. |
MLA | Wang, Liping,et al."Determination of trace elements in salt lake brines using inductively coupled plasma optical emission spectrometry after magnesium hydroxide precipitation".ANALYTICAL METHODS 7.19(2015):8235-8240. |
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