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Mixed bridged dinuclear Ni(II) complex incorporating 2-pyridinealdoxime ligand: Synthesis, crystal structure and magnetic property
Zheng, Lina1; Zhang, Suyun1; Li, Kai1; Chen, Wenqian1; Chen, Yanmei2; Xu, Bin2; Hu, Bin2; Li, Yahong1,2,3; Li, Wu2
2010-12-15
Source PublicationJOURNAL OF MOLECULAR STRUCTURE
ISSN0022-2860
Volume984Issue:1-3Pages:153-156
SubtypeArticle
AbstractA complex of the composition [Ni-2(Hpyco)(2)(ePa)(EtOH)Cl-3] (1) (Hpyco = pyridine-2-carbaldehyde oxime; Hepa = 3-(ethoxycarbonyl)picolinic acid) has been synthesized via solvothermal synthetic reaction, and fully characterized by X-ray single crystal diffraction. IR and elemental analysis. Crystal structure revealed that 1 contains carboxylic oxygen atom bridged and chloro bridged dinuclear core with each Ni(II) exhibiting pseudo-octahedral geometry. An ester was formed in situ by the reaction of solvent ethanol with one carboxylic group of pyridine-2,3-dicarboxylic acid. Low-temperature magnetic susceptibility measurement for the solid sample of 1 revealed the ferromagnetic Ni-II center dot center dot center dot Ni-II interactions. (C) 2010 Elsevier B.V. All rights reserved.
KeywordPyridine-2-carbaldehyde Oxime Mixed Bridged In Situ Reaction Magnetic Property
WOS HeadingsScience & Technology ; Physical Sciences
WOS KeywordTRANSITION-METAL-COMPLEXES ; SINGLE-MOLECULE MAGNETISM ; DINICKEL(II) COMPLEXES ; COORDINATION BEHAVIOR ; NICKEL(II) COMPLEX ; BINUCLEAR NICKEL ; PYRIDYL OXIMES ; SPIN-EXCHANGE ; CLUSTER ; CHEMISTRY
Indexed BySCI
Language英语
WOS Research AreaChemistry
WOS SubjectChemistry, Physical
WOS IDWOS:000285659400020
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Document Type期刊论文
Identifierhttp://ir.isl.ac.cn/handle/363002/1895
Collection青海盐湖研究所知识仓储
Affiliation1.Soochow Univ, Key Lab Organ Synth Jiangsu Prov, Coll Chem & Chem Engn, Suzhou 215123, Peoples R China
2.Chinese Acad Sci, Key Lab Salt Lake Resources & Chem, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China
3.Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
Recommended Citation
GB/T 7714
Zheng, Lina,Zhang, Suyun,Li, Kai,et al. Mixed bridged dinuclear Ni(II) complex incorporating 2-pyridinealdoxime ligand: Synthesis, crystal structure and magnetic property[J]. JOURNAL OF MOLECULAR STRUCTURE,2010,984(1-3):153-156.
APA Zheng, Lina.,Zhang, Suyun.,Li, Kai.,Chen, Wenqian.,Chen, Yanmei.,...&Li, Wu.(2010).Mixed bridged dinuclear Ni(II) complex incorporating 2-pyridinealdoxime ligand: Synthesis, crystal structure and magnetic property.JOURNAL OF MOLECULAR STRUCTURE,984(1-3),153-156.
MLA Zheng, Lina,et al."Mixed bridged dinuclear Ni(II) complex incorporating 2-pyridinealdoxime ligand: Synthesis, crystal structure and magnetic property".JOURNAL OF MOLECULAR STRUCTURE 984.1-3(2010):153-156.
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