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Synthesis of Mg2B2O5 whiskers via coprecipitation and sintering process
Zhu, Dong-hai1,2; Nai, Xue-ying1; Zhu, Cheng-cai1,2; Guo, Feng-qin3; Bian, Shao-ju1; Li, Wu1
2012-10-01
发表期刊INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS
ISSN1674-4799
卷号19期号:10页码:969-972
文章类型Article
摘要Mg2B2O5 whiskers with high aspect ratio were synthesized by coprecipitation and sintering process using MgCl2 center dot 6H(2)O, H3BO3, and NaOH as raw materials and KCl as a flux. Their formation process was investigated by thermogravimetry and differential scanning calorimetry (TG-DSC), X-ray diffraction (XRD), and scanning electron microcopy (SEM). It is found that the products synthesized at 832A degrees C are monoclinic Mg2B2O5 whiskers with a diameter of 200-400 nm and a length of 50-80 mu m. Transmission electron microscopy (TEM) and selected area electron diffraction (SAED) analyses show that the whiskers obtained at 832A degrees C are single crystalline and grow along with the [010] direction. The growth mechanism of Mg2B2O5 whiskers was also presented.
关键词Magnesium Borate Coprecipitation Sintering Crystal Whiskers Crystal Growth Microstructure
WOS标题词Science & Technology ; Technology ; Physical Sciences
关键词[WOS]MAGNESIUM BORATE NANORODS ; CHEMICAL-VAPOR-DEPOSITION ; MECHANISM ; GROWTH
收录类别SCI
语种英语
WOS研究方向Materials Science ; Metallurgy & Metallurgical Engineering ; Mining & Mineral Processing
WOS类目Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering ; Mining & Mineral Processing
WOS记录号WOS:000309355000015
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/2021
专题青海盐湖研究所知识仓储
盐湖资源与化学实验室
作者单位1.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
3.Qinghai Univ, Dept Basin Educ, Xining 810016, Peoples R China
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GB/T 7714
Zhu, Dong-hai,Nai, Xue-ying,Zhu, Cheng-cai,et al. Synthesis of Mg2B2O5 whiskers via coprecipitation and sintering process[J]. INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS,2012,19(10):969-972.
APA Zhu, Dong-hai,Nai, Xue-ying,Zhu, Cheng-cai,Guo, Feng-qin,Bian, Shao-ju,&Li, Wu.(2012).Synthesis of Mg2B2O5 whiskers via coprecipitation and sintering process.INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS,19(10),969-972.
MLA Zhu, Dong-hai,et al."Synthesis of Mg2B2O5 whiskers via coprecipitation and sintering process".INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS 19.10(2012):969-972.
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