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题名: Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dotH2O whiskers via a new route
作者: 刘鑫 ;  李武 ;  乃学瑛 ;  Bian, Shaoju ;  孟庆芬 ;  高丹丹 ;  魏明
刊名: CRYSTAL RESEARCH AND TECHNOLOGY
出版日期: 2012
卷号: 47, 期号:4, 页码:455-460
关键词: zinc borate ;  whisker ;  synthesis ;  flame retardant
英文摘要: 4ZnO.B2O3.H2O whiskers were prepared from 2ZnO.3B2O3.3.5H2O under hydrothermal process at 160 degrees C for 10 h. The synthesized product was characterized by XRD, SEM, TG-DSC and FT-IR. SEM results showed that the synthesized 4ZnO.B2O3.H2O whiskers' length was about 310 mu m and the diameter was 0.20.3 mu m. Further study on the whiskers' growth process and mechanism showed that the formation of the whiskers went through three stages and the morphology of 4ZnO.B2O3.H2O changed from irregular particles to rod-like structures and finally to whiskers. The variation of the morphology of the 4ZnO.B2O3.H2O whisker with the concentration of the starting material was investigated. (C) 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim) 4ZnO.B2O3.H2O whiskers were prepared from 2ZnO.3B2O3.3.5H2O under hydrothermal process at 160 degrees C for 10 h. The synthesized product was characterized by XRD, SEM, TG-DSC and FT-IR. SEM results showed that the synthesized 4ZnO.B2O3.H2O whiskers' length was about 310 mu m and the diameter was 0.20.3 mu m. Further study on the whiskers' growth process and mechanism showed that the formation of the whiskers went through three stages and the morphology of 4ZnO.B2O3.H2O changed from irregular particles to rod-like structures and finally to whiskers. The variation of the morphology of the 4ZnO.B2O3.H2O whisker with the concentration of the starting material was investigated. (C) 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)
收录类别: SCI
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内容类型: 期刊论文
URI标识: http://ir.isl.ac.cn/handle/363002/2061
Appears in Collections:青海盐湖研究所知识仓储(2014年之前)_期刊论文

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Recommended Citation:
Liu, Xin,Li, Wu,Nai, Xueying,et al. Hydrothermal synthesis and formation of 4ZnO center dot B2O3 center dotH2O whiskers via a new route[J]. CRYSTAL RESEARCH AND TECHNOLOGY,2012,47(4):455-460.
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