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题名: Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O
作者: Wang, Shoujiang ;  Mo, Shaofen ;  Liu, Zhen-Gang
刊名: RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
出版日期: 2012
卷号: 57, 期号:3, 页码:430-433
英文摘要: A new complex with the formula (NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O (1) has been synthesized and characterized by single crystal X-ray diffraction and infrared spectrum. The complex is small yellow crystal and space group P (1) with a = 9.9869(18) , b = 10.030(19) , c = 10.366(19) , alpha = 91.68(3)A degrees, beta = 98.94(3)A degrees, gamma = 119.37(2)A degrees, V = 887(3) (3), and Z = 1. The complex contains two malonic acid ligands bonded to the gamma-Mo-8 (26) (4-) ions which consist of eight MoO6 edge-sharing octahedral. In this crystal structure, the octamolybdate anion is mutually hydrogen bonded by ammonium ions and water molecules. A new complex with the formula (NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O (1) has been synthesized and characterized by single crystal X-ray diffraction and infrared spectrum. The complex is small yellow crystal and space group P (1) with a = 9.9869(18) , b = 10.030(19) , c = 10.366(19) , alpha = 91.68(3)A degrees, beta = 98.94(3)A degrees, gamma = 119.37(2)A degrees, V = 887(3) (3), and Z = 1. The complex contains two malonic acid ligands bonded to the gamma-Mo-8 (26) (4-) ions which consist of eight MoO6 edge-sharing octahedral. In this crystal structure, the octamolybdate anion is mutually hydrogen bonded by ammonium ions and water molecules.
收录类别: SCI
Citation statistics: 
内容类型: 期刊论文
URI标识: http://ir.isl.ac.cn/handle/363002/2068
Appears in Collections:青海盐湖研究所知识仓储(2014年之前)_期刊论文

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Recommended Citation:
Wang, Shoujiang,Mo, Shaofen,Liu, Zhen-Gang. Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O[J]. RUSSIAN JOURNAL OF INORGANIC CHEMISTRY,2012,57(3):430-433.
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