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Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O
Wang, Shoujiang; Mo, Shaofen; Liu, Zhen-Gang
2012
发表期刊RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
ISSN0036-0236
卷号57期号:3页码:430-433
摘要A new complex with the formula (NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O (1) has been synthesized and characterized by single crystal X-ray diffraction and infrared spectrum. The complex is small yellow crystal and space group P (1) with a = 9.9869(18) , b = 10.030(19) , c = 10.366(19) , alpha = 91.68(3)A degrees, beta = 98.94(3)A degrees, gamma = 119.37(2)A degrees, V = 887(3) (3), and Z = 1. The complex contains two malonic acid ligands bonded to the gamma-Mo-8 (26) (4-) ions which consist of eight MoO6 edge-sharing octahedral. In this crystal structure, the octamolybdate anion is mutually hydrogen bonded by ammonium ions and water molecules. A new complex with the formula (NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O (1) has been synthesized and characterized by single crystal X-ray diffraction and infrared spectrum. The complex is small yellow crystal and space group P (1) with a = 9.9869(18) , b = 10.030(19) , c = 10.366(19) , alpha = 91.68(3)A degrees, beta = 98.94(3)A degrees, gamma = 119.37(2)A degrees, V = 887(3) (3), and Z = 1. The complex contains two malonic acid ligands bonded to the gamma-Mo-8 (26) (4-) ions which consist of eight MoO6 edge-sharing octahedral. In this crystal structure, the octamolybdate anion is mutually hydrogen bonded by ammonium ions and water molecules.
收录类别SCI
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/2068
专题青海盐湖研究所知识仓储
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GB/T 7714
Wang, Shoujiang,Mo, Shaofen,Liu, Zhen-Gang. Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O[J]. RUSSIAN JOURNAL OF INORGANIC CHEMISTRY,2012,57(3):430-433.
APA Wang, Shoujiang,Mo, Shaofen,&Liu, Zhen-Gang.(2012).Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O.RUSSIAN JOURNAL OF INORGANIC CHEMISTRY,57(3),430-433.
MLA Wang, Shoujiang,et al."Synthesis and characterization of a new octamolybdate(NH4)(4)[Mo8O24(C3H2O2)(2)] center dot 4H(2)O".RUSSIAN JOURNAL OF INORGANIC CHEMISTRY 57.3(2012):430-433.
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