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Design and preparation of high-aspect-ratio zinc borate whiskers and their effects on mechanical properties of PP nanocomposite
Liu, Xin; Dang, Li; Nai, Xueying; Dong, Yaping; Li, Wu
2018-10
发表期刊RESEARCH ON CHEMICAL INTERMEDIATES
ISSN0922-6168
卷号44期号:10页码:5697-5709
摘要Well-dispersed, high-aspect-ratio 4ZnOB(2)O(3)H(2)O whiskers (4ZnOB(2)O(3)H(2)O(HARw)) were synthesized by a facile hydrothermal method with the aid of ZnSO(4)7H(2)O. The formation mechanism was investigated, and the results showed that Zn2+ and SO42- ions played a crucial role in the control of 4ZnOB(2)O(3)H(2)O(HARw) extended along [010] direction. X-ray diffraction (XRD) analysis, high-resolution transmission electron microscopy (HR-TEM), X-ray photoelectron spectroscopy (XPS), and thermogravimetry (TG)-differential scanning calorimetry (DSC) results confirmed that the powder was 4ZnOB(2)O(3)H(2)O. Scanning electron microscopy (SEM) and TEM showed that the average aspect ratio of the product was about 100. Nanocomposites of surface-modified 4ZnOB(2)O(3)H(2)O(SM-HARw)/PP were prepared and their mechanical properties measured. The results suggested that the mechanical properties of 4ZnOB(2)O(3)H(2)O(SM-HARw)/PP composites were superior to composites made with low-aspect-ratio whiskers (4ZnOB(2)O(3)H(2)O(SM-LARw)), which displayed poorer mechanical properties even at low addition.
DOI10.1007/s11164-018-3450-9
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文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/34452
专题盐湖资源综合利用工程技术中心
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Liu, Xin,Dang, Li,Nai, Xueying,et al. Design and preparation of high-aspect-ratio zinc borate whiskers and their effects on mechanical properties of PP nanocomposite[J]. RESEARCH ON CHEMICAL INTERMEDIATES,2018,44(10):5697-5709.
APA Liu, Xin,Dang, Li,Nai, Xueying,Dong, Yaping,&Li, Wu.(2018).Design and preparation of high-aspect-ratio zinc borate whiskers and their effects on mechanical properties of PP nanocomposite.RESEARCH ON CHEMICAL INTERMEDIATES,44(10),5697-5709.
MLA Liu, Xin,et al."Design and preparation of high-aspect-ratio zinc borate whiskers and their effects on mechanical properties of PP nanocomposite".RESEARCH ON CHEMICAL INTERMEDIATES 44.10(2018):5697-5709.
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