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Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process
Wu Jian-Song1; Xiao Ying-Kai2; Chen Lang-Yin1; Chen Xiao-Wei1
2009-12-10
发表期刊CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
卷号30期号:12页码:2354-2357
文章类型Article
摘要The magnesium hydroxide whisker with excellent quality was synthesized by glycerol-frequency conversion microwave-hydrothermal process with MgCl(2) center dot 6H(2)O and NaOH as raw materials. The phase, granularity, structure of crystal morphology of whiskers samples were characterized by X-ray diffraction (XRD), scanning electron microscop ( SEM) and transmission electron microscop ( TEM). The effect of glycerol-frequency conversion microwave-hydrothermal process on the crystal form, Structure, and dispersive capability of magnesium hydroxide whisker was investigated. The results show that high quality magnesium hydroxide whiskers with symmetrical granularity, fine crystal form and dispersibility, glabrous surface, as well as little crystal defect. are obtained when 15% ( volume fraction) of glycerol is added and heated at 180 degrees C for 6 h. The TEM images show that the diameters of whiskers are about 0.1-0.3 mu m and the length are about 80-110 mu m. The influence of glycerol and frequency conversion microwave on growth of magnesium hydroxide whiskeres was investigated primarily.
关键词Frequency Conversion Microwave Glycerol Hydrothermal Method Magnesium Hydroxide Whisker
WOS标题词Science & Technology ; Physical Sciences
关键词[WOS]SULFATE HYDRATE ; ZNO ; GROWTH
收录类别SCI
语种英语
WOS研究方向Chemistry
WOS类目Chemistry, Multidisciplinary
WOS记录号WOS:000273792900005
引用统计
被引频次:5[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/5905
专题青海盐湖研究所知识仓储
作者单位1.Zhanjiang Normal Univ, Chem Sci & Technol Sch, Zhanjiang 524048, Peoples R China
2.Chinese Acad Sci, Inst Salt Lakes, Key Lab Salt Lake Resources & Chem, Xining 810008, Peoples R China
推荐引用方式
GB/T 7714
Wu Jian-Song,Xiao Ying-Kai,Chen Lang-Yin,et al. Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2009,30(12):2354-2357.
APA Wu Jian-Song,Xiao Ying-Kai,Chen Lang-Yin,&Chen Xiao-Wei.(2009).Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,30(12),2354-2357.
MLA Wu Jian-Song,et al."Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 30.12(2009):2354-2357.
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