Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process

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	Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process
	Wu Jian-Song 1; Xiao Ying-Kai 2; Chen Lang-Yin 1; Chen Xiao-Wei 1
	2009-12-10
发表期刊	CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
卷号	30 期号:12 页码:2354-2357
关键词	Frequency Conversion Microwave Glycerol Hydrothermal Method Magnesium Hydroxide Whisker
摘要	The magnesium hydroxide whisker with excellent quality was synthesized by glycerol-frequency conversion microwave-hydrothermal process with MgCl(2) center dot 6H(2)O and NaOH as raw materials. The phase, granularity, structure of crystal morphology of whiskers samples were characterized by X-ray diffraction (XRD), scanning electron microscop ( SEM) and transmission electron microscop ( TEM). The effect of glycerol-frequency conversion microwave-hydrothermal process on the crystal form, Structure, and dispersive capability of magnesium hydroxide whisker was investigated. The results show that high quality magnesium hydroxide whiskers with symmetrical granularity, fine crystal form and dispersibility, glabrous surface, as well as little crystal defect. are obtained when 15% ( volume fraction) of glycerol is added and heated at 180 degrees C for 6 h. The TEM images show that the diameters of whiskers are about 0.1-0.3 mu m and the length are about 80-110 mu m. The influence of glycerol and frequency conversion microwave on growth of magnesium hydroxide whiskeres was investigated primarily.
语种	英语
引用统计
文献类型	期刊论文
条目标识符	http://ir.isl.ac.cn/handle/363002/5905
专题	青海盐湖研究所知识仓储中国科学院青海盐湖研究所
作者单位	1.Zhanjiang Normal Univ, Chem Sci & Technol Sch, Zhanjiang 524048, Peoples R China 2.Chinese Acad Sci, Inst Salt Lakes, Key Lab Salt Lake Resources & Chem, Xining 810008, Peoples R China
推荐引用方式 GB/T 7714	Wu Jian-Song,Xiao Ying-Kai,Chen Lang-Yin,et al. Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2009,30(12):2354-2357.
APA	Wu Jian-Song,Xiao Ying-Kai,Chen Lang-Yin,&Chen Xiao-Wei.(2009).Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,30(12),2354-2357.
MLA	Wu Jian-Song,et al."Preparation of Magnesium Hydroxide Whisker by Glycerol-Frequency Conversion Microwave-Hydrothermal Process".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 30.12(2009):2354-2357.