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Effective elimination of organic matter interference in boron isotopic analysis by thermal ionization mass spectrometry of coral/foraminifera: micro-sublimation technology combined with ion exchange
He, Maoyong1,2; Xiao, Yingkai2; Ma, Yunqi2; Jin, Zhangdong1; Xiao, Jun1
2011-03-30
发表期刊RAPID COMMUNICATIONS IN MASS SPECTROMETRY
卷号25期号:6页码:743-749
文章类型Article
摘要In order to better estimate the effectiveness of micro-sublimation technology on the elimination of organic matter interference during boron isotopic analysis, a series of improved experiments was carried out using simple apparatus. Recovery rates after micro-sublimation were measured for boric acid solutions with different B contents or different B/organic matter ratios. The improved micro-sublimation procedure combined with ion-exchange technology was then used to test natural samples (coral and foraminifera) for the separation of boron. Our results show that the time taken for 100% recovery of different amounts of B differed and that the proportions of B/organic matter within the natural organic matter have little effect on the relationship between the recovery rates of B and the micro-sublimation times. The experiments further confirm that the organic matter does indeed have an effect on boron isotope analyses by positive thermal ionization mass spectrometry and that the use of micro-sublimation can effectively remove interferences from the organic matter during boron isotopic analysis. Copyright (C) 2011 John Wiley & Sons, Ltd.
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences ; Technology
关键词[WOS]SURFACE OCEAN PH ; FRACTIONATION ; CARBONATES ; SKELETAL ; RATIOS ; ACID
收录类别SCI
语种英语
WOS研究方向Biochemistry & Molecular Biology ; Chemistry ; Spectroscopy
WOS类目Biochemical Research Methods ; Chemistry, Analytical ; Spectroscopy
WOS记录号WOS:000287596300008
引用统计
被引频次:6[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/5988
专题青海盐湖研究所知识仓储
作者单位1.Chinese Acad Sci, Inst Earth Environm, State Key Lab Loess & Quaternary Geol, Xian 710075, Peoples R China
2.Chinese Acad Sci, Qinghai Inst Salt Lakes, CAS Key Lab Salt Lake Resources & Chem, Xining 810008, Peoples R China
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He, Maoyong,Xiao, Yingkai,Ma, Yunqi,et al. Effective elimination of organic matter interference in boron isotopic analysis by thermal ionization mass spectrometry of coral/foraminifera: micro-sublimation technology combined with ion exchange[J]. RAPID COMMUNICATIONS IN MASS SPECTROMETRY,2011,25(6):743-749.
APA He, Maoyong,Xiao, Yingkai,Ma, Yunqi,Jin, Zhangdong,&Xiao, Jun.(2011).Effective elimination of organic matter interference in boron isotopic analysis by thermal ionization mass spectrometry of coral/foraminifera: micro-sublimation technology combined with ion exchange.RAPID COMMUNICATIONS IN MASS SPECTROMETRY,25(6),743-749.
MLA He, Maoyong,et al."Effective elimination of organic matter interference in boron isotopic analysis by thermal ionization mass spectrometry of coral/foraminifera: micro-sublimation technology combined with ion exchange".RAPID COMMUNICATIONS IN MASS SPECTROMETRY 25.6(2011):743-749.
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