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Kinetics of synthetic of Cl- type hydrotalcitelike with coprecipitation reaction
Gou, GJ; Ma, PH; Chu, MX
2004-11-01
发表期刊ACTA PHYSICO-CHIMICA SINICA
卷号20期号:11页码:1357-1363
文章类型Article
摘要The dynamics feature and mechanism of preparation of layered double hydroxides pillared by Cl- anion (LDH-Cl) with coprecipitation reaction had been investigated, based on the result of monitoring concentrations during reaction course, and on the result of EDS, IR, XRD, TEM and TG-DTA characterization for samples produced from different reaction course. The results testified that the generating of LDH-Cl was controlled by polynuclcar layer surface reaction mechanism. It was also found that the lattice parameter c decreased from 2. 421 nm to 2. 399 nm, and h from 0. 3321 nm to 0. 3228 nm, with grain size increasing of D-a from 6. 40 nm to 15. 16 nm, D. from 7. 43 nm to 10. 93 nm, and increasing of aspect ratio from 0. 86 to 1. 39 during the whole reaction course, in addition, the strength of interaction between sheet and anions and the structure stability of sheet enhancing with reaction course as showed by IR and TG-DTA characterization.
关键词Layered Double Hydroxides Pillared By Cl- (Ldh-cl) Coprecipitation Reaction Course
WOS标题词Science & Technology ; Physical Sciences
关键词[WOS]CRYSTAL-STRUCTURE ; HYDROXIDE
收录类别SCI
语种英语
WOS研究方向Chemistry
WOS类目Chemistry, Physical
WOS记录号WOS:000225381400014
引用统计
被引频次:10[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/6123
专题青海盐湖研究所知识仓储
作者单位1.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
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Gou, GJ,Ma, PH,Chu, MX. Kinetics of synthetic of Cl- type hydrotalcitelike with coprecipitation reaction[J]. ACTA PHYSICO-CHIMICA SINICA,2004,20(11):1357-1363.
APA Gou, GJ,Ma, PH,&Chu, MX.(2004).Kinetics of synthetic of Cl- type hydrotalcitelike with coprecipitation reaction.ACTA PHYSICO-CHIMICA SINICA,20(11),1357-1363.
MLA Gou, GJ,et al."Kinetics of synthetic of Cl- type hydrotalcitelike with coprecipitation reaction".ACTA PHYSICO-CHIMICA SINICA 20.11(2004):1357-1363.
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