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Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process
Zhu Donghai1,2; Nai Xueying2; Lan Shengjie1,3; Dang Li1,3; Liu Xin2; Li Wu2
2017-10-01
发表期刊JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
卷号32期号:5页码:1067-1071
文章类型Article
摘要Single crystalline calcium chloroborate (Ca2B5O9Cl) whiskers with uniform diameter have been fabricated by a two-step process. The precursor was firstly prepared by the sedimentation reaction between CaCl2, H3BO3 and NaOH aqueous solutions, and then sintered at different temperatures for 6 h with KCl as flux. The XRD indicates that the product synthesized at 600 degrees C is Orthorhombic Ca2B5O9Cl. SEM and TEM results show that the Ca2B5O9Cl is whisker with the diameter about 0.2-0.5 mu m and the length up to 15 mu m. SAED analysis shows that the whisker is single crystalline and grows along [001] direction. The possible formation process and growth mechanism were proposed.
关键词Single Crystal Growth Ca2b5o9cl Whiskers Microstructures
WOS标题词Science & Technology ; Technology
关键词[WOS]ALUMINUM BORATE WHISKERS ; MECHANICAL-PROPERTIES ; COMPOSITES ; BEHAVIORS
收录类别SCI
语种英语
WOS研究方向Materials Science
WOS类目Materials Science, Multidisciplinary
WOS记录号WOS:000412950000013
引用统计
文献类型期刊论文
条目标识符http://ir.isl.ac.cn/handle/363002/6261
专题青海盐湖研究所知识仓储
盐湖资源综合利用工程技术中心
作者单位1.Qinghai Univ, State Key Lab Plateau Ecol & Agr, Xining 810016, Qinghai, Peoples R China
2.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China
3.Qinghai Univ, Sch Chem Engn, Xining 810016, Qinghai, Peoples R China
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GB/T 7714
Zhu Donghai,Nai Xueying,Lan Shengjie,et al. Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2017,32(5):1067-1071.
APA Zhu Donghai,Nai Xueying,Lan Shengjie,Dang Li,Liu Xin,&Li Wu.(2017).Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,32(5),1067-1071.
MLA Zhu Donghai,et al."Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 32.5(2017):1067-1071.
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