ISL OpenIR  > 青海盐湖研究所知识仓储
Facile synthesis of Co3O4 hexagonal plates by flux method
Han, Ji-Long1; Meng, Qing-Fen1; Gao, Sheng-Li2
2018-01-15
Source PublicationJOURNAL OF CRYSTAL GROWTH
Volume482Pages:23-29
SubtypeArticle
AbstractUsing a novel flux method, a hexagonal plate of Co3O4 was directly synthesized. In this method, CoCl2 center dot 6H(2)O, NaOH, and the cosolvent H3BO3 were heated to 750 degrees C for 2 h in a corundum crucible. The products were characterized with X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and high-resolution transmission electron microscope (HRTEM). Furthermore, XRD studies indicated that the product consisted of a cubic phase of Co3O4, and the phase existed in a completely crystalline form. Then, SEM results indicated that these hexagonal plates tiered up and they had diameters in the range of 210 mu m. According to the results of SAED and HRTEM analyses, the interlayer spacing was about 0.24 nm, which corresponds to the interlayer distance of (3 1 1) crystal plane of cubic Co3O4. (C) 2017 Elsevier B.V. All rights reserved.
KeywordCrystal Morphology Growth From Melt Flux Method Oxides
WOS HeadingsScience & Technology ; Physical Sciences ; Technology
WOS KeywordLITHIUM-ION BATTERIES ; MOLTEN-SALT SYNTHESIS ; LI-STORAGE ; NANOPARTICLES ; NANORODS ; CATHODE ; NANOFIBERS ; NANOCUBES ; PROPERTY ; SURFACE
Indexed BySCI
Language英语
WOS Research AreaCrystallography ; Materials Science ; Physics
WOS SubjectCrystallography ; Materials Science, Multidisciplinary ; Physics, Applied
WOS IDWOS:000415307000004
Citation statistics
Document Type期刊论文
Identifierhttp://ir.isl.ac.cn/handle/363002/6405
Collection青海盐湖研究所知识仓储
盐湖地质与环境实验室
Affiliation1.Chinese Acad Sci, Qinghai Inst Salt Lakes, Key Lab Comprehens & Highly Efficient Utilizat Sa, Xining 810008, Qinghai, Peoples R China
2.Northwest Univ, Coll Chem & Mat Sci, Key Lab Synthet & Nat Funct Mol Chem, Minist Educ, Xian 710069, Shaanxi, Peoples R China
Recommended Citation
GB/T 7714
Han, Ji-Long,Meng, Qing-Fen,Gao, Sheng-Li. Facile synthesis of Co3O4 hexagonal plates by flux method[J]. JOURNAL OF CRYSTAL GROWTH,2018,482:23-29.
APA Han, Ji-Long,Meng, Qing-Fen,&Gao, Sheng-Li.(2018).Facile synthesis of Co3O4 hexagonal plates by flux method.JOURNAL OF CRYSTAL GROWTH,482,23-29.
MLA Han, Ji-Long,et al."Facile synthesis of Co3O4 hexagonal plates by flux method".JOURNAL OF CRYSTAL GROWTH 482(2018):23-29.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Han, Ji-Long]'s Articles
[Meng, Qing-Fen]'s Articles
[Gao, Sheng-Li]'s Articles
Baidu academic
Similar articles in Baidu academic
[Han, Ji-Long]'s Articles
[Meng, Qing-Fen]'s Articles
[Gao, Sheng-Li]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Han, Ji-Long]'s Articles
[Meng, Qing-Fen]'s Articles
[Gao, Sheng-Li]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.